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Please use this identifier to cite or link to this item: http://hdl.handle.net/123456789/4219

Title: Preparation and characterization of new in(iii), re(iii), and re(v) complexes with thenoyltrifluoroacetone and some bidentate heterocyclic ligands
Authors: Mahfouz, Refaat M.
Al-Farhan, Khalid A.
Hassen, Gamila Y.
Al-Wassil, Abdulaziz I.
Alshehri, Saad M.
Al-Wallan, Ami A.
Keywords: NEW In(III)
Thenoyltrifluoroacetone
Bidentate
Heterocyclic
Ligands
Issue Date: 2002
Citation: Synth. React. Inorg. Met. Org. Chem: 32 (3); 489-508
Abstract: All chemical used were of analytical grade and were used without further purification. IR spectra were recorded in KBr pellets on a Perkin Elmer FT-IR spectrometer. "Spectrum 1000". UV-Vis spectra in ethanolic solutions were recorded on a Cecil 599 spectrophotometer using 1 cm matched silica cells. 'H and , 3 C NMR spectra were measured in DMSO-d6 as solvent on a JEOL NMR 400 MHZ spectrometer. Elemental analyses were carried out on a Perkin Elmer 2400 CHNSO elemental analyzer. Iidium contents in the investigated indium complexes were determined by the analytical laboratory at SABIC (R&D) (Saudi Arabia). TG measurements were carried out using a Netzsch STA-429 thermal analyzer. The weight loss was measured from ambient temperature up to 700 °C'at a heating rate of 10 °C/min. X-ray diffraction patterns of the complexes were recorded using a XRD 5000 Siemens diffractometer with Cu-target.
URI: http://hdl.handle.net/123456789/4219
Appears in Collections:College of Science

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